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Synthesis of 1,3-bis(4,5-dihydrothiazole) benzene

Article type: Research Article

Authors: Atwood, D.A. | Delcamp, J. | Zaman, M.K.

Affiliations: University of Kentucky, Lexington, KY, USA

Note: [] Corresponding author. E-mail: datwood@pop.uky.edu

Abstract: A new compound, 1,3-bis(4,5-dihydrothiazole) benzene was synthesized by refluxing benzene-1,3-diamidoethanethiol (BDETH2) in toluene in the presence of trimethylaluminum. The compound was characterized by IR, NMR, Mass spectroscopy, Elemental Analysis, and X-ray crystallography.

Keywords: BDETH2, Trimethylaluminum, Cyclization

DOI: 10.1080/10241220600888350

Journal: Main Group Chemistry, vol. 5, no. 2, pp. 137-140, 2006

Received 10 June 2006
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Published: 2006
Price: EUR 27.50
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