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Article type: Research Article
Authors: Hauback, Bjørn C. | FjellvåG, Helmer | Steinsvoll, Olav | Johansson, Kjell | Buset, Ole Tore | Jørgensen, Johny
Affiliations: Institute for Energy Technology, N-2027 Kjeller, Norway | Department of Chemistry, University of Oslo, N-0315 Oslo, Norway
Note: [] Corresponding author. Department of Physics, Institute for Energy Technology, P.O. Box 40, N-2027 Kjeller, Norway. Fax: +47 63 81 09 20. E-mail: bjorn@ife.no
Abstract: The performance of the new Powder Neutron Diffractometer PUS at the 2 MW JEEP II reactor shows the large potential for high resolution powder neutron diffraction even at a low flux reactor. The different components of the instrument are optimised with respect to flexibility and relationship between intensity and resolution. Wavelengths in the range 0.7–2.6 Å are available from a focussing composite Ge monochromator. The detector system consists of position sensitive proportional counters. The temperatures available for experiments range from 7 to about 1600 K. Nearly no malfunctions during the first 2 1/2 years of operation proves the robustness of the complete system. Several experiments show the potential for studies of rather complex crystallographic problems, even with small sample quantities (<200 mg), and timeresolved in-situ type experiments.
Keywords: Neutron diffraction, Powder diffraction, Diffractometer
DOI: 10.1080/10238160008200055
Journal: Journal of Neutron Research, vol. 8, no. 3, pp. 215-232, 2000
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